Synthesis and structure of {[}1,2]thiaphospholo{[}4,5-e]{[}1,2,4]triazines

Faculty Pharmacy Year: 1999
Type of Publication: Article Pages: 13457-13462
Authors:
KADRY, AM, IBRAHIM, YA, Ibrahim, MR, Lisgarten, JN, Potter, BS, Palmer, RA
DOI: 10.1016/S0040-4020(99)00830-3
Journal: TETRAHEDRON PERGAMON-ELSEVIER SCIENCE LTD Volume: 55
Research Area: Chemistry ISSN ISI:000083407900012
Keywords : Synthesis , structure , {[}1,2]thiaphospholo{[}4,5-e]{[}1,2,4]triazines    
Abstract:
The first syntheses of the novel {[}1,2]thiaphospholo{[}4,5-e]{[}1,2,4]triazine ring system, exemplified by the derivatives 3a-c have been accomplished by the action of Lawesson's reagent on the 5-arylmethyl-1,2,4-triazin-6-ones 1a-c, their thiones 2a-c or the Mannich bases 4-6. The structure of these new thiaphospholotriazines was established mainly by NMR, and X-ray structural analysis. (C) 1999 Elsevier Science Ltd. All rights reserved.
    
  Online    
PDF  
       
Tweet