Synthesis and characterization of V(III), Cr(III) and Fe(III) hippurates

Faculty	Science	Year:	2005
Type of Publication:	Article	Pages:	139-145
Authors:	SADEEK, SA, TELEB, SM, Refat, MS, El-Megharbel, SM	DOI:	10.1016/j.molstruc.2004.10.017
Journal:	JOURNAL OF MOLECULAR STRUCTURE ELSEVIER SCIENCE BV	Volume:	737
Research Area:	Chemistry	ISSN	ISI:000227082800009
Keywords :	electronic spectra, hippuric acid, H-1 NMR, TGA
Abstract:	Hippurates of V(III), Cr(III) and Fe(III) were isolated as solids with the general formula; {[}V(hip)(3)].15H(2)O, {[}Cr(hip)(3)].6H(2)O and {[}Fe(hip)(3)].1.5H(2)O. The compounds were characterized from elemental analysis, infrared spectra, H-1 NMR, electronic spectra and thermogravimetric analysis and proof that metal-ligand coordination involves only via the carboxylate group. (C) 2004 Elsevier B.V. All rights reserved.
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