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Vibrational and thermal studies of the complexes (NH4){[}VO(O-2)(2)(phen)]center dot 2H(2)O and (NH4){[}V(O-2)(3)(phen)]center dot 2H(2)O
Faculty
Specific Education
Year:
2005
Type of Publication:
Article
Pages:
814-818
Authors:
TELEB, SM, Gaballa, AS, Barakat, AS, Mohammed, SF
DOI:
10.1016/j.saa.2005.03.009
Journal:
SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY PERGAMON-ELSEVIER SCIENCE LTD
Volume:
62
Research Area:
Spectroscopy
ISSN
ISI:000233930600008
Keywords :
oxodiperoxo and triperoxo, IR, thermal analyses
Abstract:
The infrared spectra of the oxodiperoxo and triperoxo complexes, (NH4){[}VO(O-2)(2)(phen)]-2H(2)O and (NH4){[}V(O-2)(3)(phen)]-2H(2)O have been recorded and the observed bands are assigned on the basis of C, symmetry. Thermogravimetric (TG) and differential thermal analysis (DTA) measurements on these two complexes were also carried out. A detailed mechanism for the mode of thermal decomposition of the two complexes has been given and supported by infrared spectral measurements on the thermal decomposition products. The data obtained agree quite well with the expected structure and indicate that the final thermal decomposition product of these two complexes is V2O5. (c) 2005 Elsevier B.V. All rights reserved.
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