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Some reactions of 4,6-diaminopyrimidinethione
Faculty
Science
Year:
2008
Type of Publication:
Article
Pages:
69-73
Authors:
Ahmed, Gamal A
DOI:
10.1080/10426500701556981
Journal:
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS TAYLOR \& FRANCIS LTD
Volume:
183
Research Area:
Chemistry
ISSN
ISI:000252850600007
Keywords :
tetrazopyrimidinethione, triazolopyridine, polynuclear heterocycle
Abstract:
Reaction of 4,6-diamino-2(1H)-pyrimidinethione (1) with p-toluene-sulfonyl hydrazine, nitrous acid and carbon disulfide afforded the compounds (2, 3) and (4) respectively. Compound (3) easily reacted with anthranilic acid, semicarbazide thiosemicarbazide and acid hydrazides and gave the polynuclearheterocyclic compounds (5, 6(a,b)) and (8(a,b)) respectively. Also, compound (4) yielded the tricyclic compound 7 when reacted with ethylchloroformate. The purpose of this article is synthesis of biologically active polynuclear heterocyclic compounds.
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