Zagazig University Digital Repository
Home
Thesis & Publications
All Contents
Publications
Thesis
Graduation Projects
Research Area
Research Area Reports
Search by Research Area
Universities Thesis
ACADEMIC Links
ACADEMIC RESEARCH
Zagazig University Authors
Africa Research Statistics
Google Scholar
Research Gate
Researcher ID
CrossRef
Synthesis, spectroscopic properties, and antimicrobial activity of some new 5-phenylazo-6-aminouracil-vanadyl complexes
Faculty
Specific Education
Year:
2011
Type of Publication:
Article
Pages:
4225-4243
Authors:
Gaballa, Akmal S, Teleb, Said M, Asker, Mohsen S, Yalcin, Ergin, Seferoglu, Zeynel
DOI:
10.1080/00958972.2011.637554
Journal:
JOURNAL OF COORDINATION CHEMISTRY TAYLOR \& FRANCIS LTD
Volume:
64
Research Area:
Chemistry
ISSN
ISI:000305485000001
Keywords :
5-Phenylazo-6-aminouracils-VO2+ complexes, IR, Thermal analysis, H-1 NMR, Antimicrobial activity
Abstract:
Six complexes, {[}VO(L-1-H)(2)]center dot 5H(2)O (1), {[}VO(OH)(L-2,L-3-H)(H2O)]center dot H2O (2,3), {[}VO(OH) (L-4,L-5-H)(H2O)]center dot H2O (4,5), {[}VO(OH)(L-6-H)(H2O)]center dot H2O (6), were prepared by reacting different derivatives of 5-phenylazo-6-aminouracil ligands with VOSO4 center dot 5H(2)O. The infrared and H-1 NMR spectra of the complexes have been assigned. Thermogravimetric analyses (TG, DTG) were also carried out. The data agree quite well with the proposed structures and show that the complexes were finally decomposed to the corresponding divanadium pentoxide. The ligands and their vanadyl complexes were screened for antimicrobial activities by the agarwell diffusion technique using DMSO as solvent. The minimum inhibitory concentration (MIC) values for 1-4 and 6 were calculated at 30 degrees C for 24-48 h. The activity data show that the complexes are more potent antimicrobials than the parent ligands.
Online
PDF
جامعة المنصورة
جامعة الاسكندرية
جامعة القاهرة
جامعة سوهاج
جامعة الفيوم
جامعة بنها
جامعة دمياط
جامعة بورسعيد
جامعة حلوان
جامعة السويس
شراقوة
جامعة المنيا
جامعة دمنهور
جامعة المنوفية
جامعة أسوان
جامعة جنوب الوادى
جامعة قناة السويس
جامعة عين شمس
جامعة أسيوط
جامعة كفر الشيخ
جامعة السادات
جامعة طنطا
جامعة بنى سويف