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Quantitative HPLC analysis of mebeverine, mesalazine, sulphasalazine and dispersible aspirin stored in a Venalink monitored dosage system with co-prescribed medicines
Faculty
Not Specified
Year:
2011
Type of Publication:
Article
Pages:
646-652
Authors:
Elmasry, Manal S, Blagbrough, Ian S, Rowan, Michael G, Saleh, Hanaa M, Kheir, Afaf Aboul, Rogers, Philip J
DOI:
10.1016/j.jpba.2010.10.002
Journal:
JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS ELSEVIER SCIENCE BV
Volume:
54
Research Area:
Chemistry; Pharmacology \& Pharmacy
ISSN
ISI:000286351200003
Keywords :
5-Aminosalicylic acid, Aspirin, Mebeverine, Mesalazine, Sulphasalazine
Abstract:
An HPLC method for the quantitative analysis of mebeverine HCl, 5-aminosalicylic acid (5-ASA), sulphasalazine and dispersible aspirin has been developed and then applied to these specific medicines when stored, with other medications, in Venalink blister packs (monitored dosage system) for periods of up to 35 days. Chromatographic separation was achieved on a reversed-phase C(12) column with an isocratic mixture of methanol, water and acetic acid as the mobile phase. The method was validated regarding: accuracy, precision, detection limits, quantification limits, specificity and robustness. (C) 2010 Elsevier B.V. All rights reserved.
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