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POLAROGRAPHIC AND CYCLIC VOLTAMMETRIC BEHAVIOR OF SOME AZO-COMPOUNDS DERIVED FROM SULFONAMIDE IN DMF AQUEOUS-SOLUTIONS
Faculty
Science
Year:
1992
Type of Publication:
Article
Pages:
268-275
Authors:
KILLA, HM, MABROUK, EM, YASEN, SA, FATTAH, AFAA
DOI:
10.1135/cccc19920268
Journal:
COLLECTION OF CZECHOSLOVAK CHEMICAL COMMUNICATIONS INST ORGANIC CHEM AND BIOCHEM
Volume:
57
Research Area:
Chemistry
ISSN
ISI:A1992HH76500007
Keywords :
POLAROGRAPHIC , CYCLIC VOLTAMMETRIC BEHAVIOR , SOME AZO-COMPOUNDS
Abstract:
The polarographic and cyclic voltammetric behaviour of (2-hydroxyphenylazo)-4-benzene-sulfonamide and some of its derivatives have been studied in Britton-Robinson buffer series containing 30 vol. \% of DMF. Over the entire pH range (2-12), the reduction pathway occurs through an irreversible 4-electron step corresponding to the reduction of N = N center to the amine stage. The voltammograms recorded in acidic and alkaline solution at different scan rates exhibit one or two cathodic peaks depending on the substituent and the pH of the medium. The electrode reaction mechanism was suggested, also the kinetic parameters were calculated.
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