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Synthesis and Characterization of
Faculty
Science
Year:
2004
Type of Publication:
Theses
Pages:
Authors:
Nermin EL Sayed Abdel Moneem
BibID
3201990
Keywords :
Alkyl Sulfosuccinate derivatives
Abstract:
Dioctyl sulfosuccinate was prepared by reaction of sulfosuccinic acid with octyl alcohol, where this compound could be used to manufacture of many different chemical compounds and it is commonly used in the industry, but its high krafft point + 6oC makes The chemical structures of the prepared surfactants were confirmed by FTIR and H1NMR spectroscopy.The surface tension of the sythesized surfactants was measured at 25, 35, 45 and 55oC, also the surface active properties were calculated, also thermodynamic micellization and adsorption of these surfactants were calculated.A series of surfactant and E(14)SMOSS, E(14)SMLSS E(14)SMCSS will chosen to form mixture with SDOSS with different molar ratios to form anionic - nonionic surfactants moities. The surface tension of the synthesized surfactants was measured at 25oC individDepending on the criticle micelle concentration values for each surfactant individually and in mixed systems, the minimum surface tension was exhibited at mixture of (0.6 SDOSS) and 0.4 E(14)SMCSS. The micellar composition of the mixed aggregated were expThe novel derivatives E(n) SMASS were examined as oil spill dispersants. The obtained results showed that, these derivatives can be used as oil spill dispersant formulation.
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